In this study, Fe-oxide-based NPs (Fe2O3 NPs) were prepared via precipitation strategy, and characterized by transmission electron microscopy (TEM), X-ray diffraction spectroscopy (XRD), X-ray photo-reduction spectroscopy (XPS), cyclic voltammetry (CV). The characterization data indicated that prepared Fe-based NPs possessed α-Fe2O3 phase with 50-60 nm diameter. Next, the CV technique was employed to test the ability of the prepared Fe2O3 NPs toward electrochemical oxidation of salicylaldehyde at a glassy carbon electrode (3 mm diameter) in an alkaline electrolyte. The results demonstrated that the electrochemical oxidation of salicylaldehyde followed first-order kinetics with a hydroxyl-radical aided process, requiring 18.4 kJ/mol activation energy at ambient temperature.
Kaur,J. and Das,D. Kumar (2024). Iron Oxide Nanoparticles-assisted Electrochemical Oxidation of Salicylaldehyde. Analytical and Bioanalytical Electrochemistry, 16(4), 307-314. doi: 10.22034/abec.2024.712919
MLA
Kaur,J. , and Das,D. Kumar. "Iron Oxide Nanoparticles-assisted Electrochemical Oxidation of Salicylaldehyde", Analytical and Bioanalytical Electrochemistry, 16, 4, 2024, 307-314. doi: 10.22034/abec.2024.712919
HARVARD
Kaur J., Das D. Kumar (2024). 'Iron Oxide Nanoparticles-assisted Electrochemical Oxidation of Salicylaldehyde', Analytical and Bioanalytical Electrochemistry, 16(4), pp. 307-314. doi: 10.22034/abec.2024.712919
CHICAGO
J. Kaur and D. Kumar Das, "Iron Oxide Nanoparticles-assisted Electrochemical Oxidation of Salicylaldehyde," Analytical and Bioanalytical Electrochemistry, 16 4 (2024): 307-314, doi: 10.22034/abec.2024.712919
VANCOUVER
Kaur J., Das D. Kumar Iron Oxide Nanoparticles-assisted Electrochemical Oxidation of Salicylaldehyde. Anal. Bioanal. Electrochem., 2024; 16(4): 307-314. doi: 10.22034/abec.2024.712919
